Carbon Capture Process Development & Automated Testing Platform

Custom automation, process development, and experimental testing systems accelerating next-generation direct air carbon capture technologies

Capabilities Demonstrated

  • Carbon capture process development
  • Automated testing platform design
  • Process scale-up engineering
  • Experimental automation systems
  • Data acquisition and analysis
  • Custom gas exchange enclosure design
  • Pneumatic automation systems
  • Environmental monitoring integration
  • Sensor evaluation and validation
  • Industrial controls development
  • Rapid prototyping and process optimization
  • Renewable energy technology development

The Challenge

As organizations seek scalable solutions to remove carbon dioxide directly from the atmosphere, one of the largest challenges is moving promising laboratory research into practical, repeatable, and scalable industrial processes.

Heirloom Carbon had developed a proprietary carbon capture process that utilized naturally occurring powdered materials capable of absorbing atmospheric CO₂ through simple oxidation reactions. By introducing controlled amounts of moisture to these materials, carbon dioxide could be captured and stored through naturally occurring chemical processes.

While initial research had demonstrated the viability of the concept, testing was largely confined to small-scale university laboratory environments. Experimental procedures were highly manual, throughput was limited, and the process lacked the automation and repeatability needed to rapidly evaluate multiple variables and accelerate development.

The organization needed a testing platform that could increase experimental throughput, improve consistency, automate data collection, and provide a pathway toward future production-scale implementation. At the same time, capital expenditures needed to remain low while the technology continued to mature and key process parameters were still being defined.

Approach

Re:Build DAPR worked closely with the Heirloom team to understand the carbon capture process, identify critical testing variables, and develop a scalable experimental platform capable of supporting accelerated process development.

The project focused on creating an automated testing environment that would allow multiple process configurations to be evaluated simultaneously while reducing manual intervention and improving data consistency. The team evaluated commercially available sensors, monitoring equipment, and environmental measurement technologies to identify cost-effective solutions capable of supporting the evolving research effort.

Research included evaluating moisture sensors, carbon dioxide sensors, carbon monoxide sensors, relative humidity instrumentation, and specialized analytical equipment used to quantify carbon content and process performance. The team also assessed methods for automating powder wetting, environmental control, gas exchange measurement, and data collection.

Recognizing the client’s need to minimize upfront investment, the initial system incorporated lower-cost commercial components where appropriate while maintaining the flexibility to evolve toward more industrialized solutions as the technology matured.

Solution

Re:Build DAPR developed an automated carbon capture testing platform designed to increase testing frequency, improve repeatability, and accelerate process development efforts.

  • Key capabilities included:
  • Automated powder wetting and testing systems
  • Custom gas exchange enclosure design
  • Environmental monitoring and sensing integration
  • CO₂, CO, moisture, and humidity measurement systems
  • Pneumatic automation systems
  • Data acquisition and logging architecture
  • Remote monitoring capabilities
  • Experimental process automation
  • Data analysis and visualization tools
  • Scalable testing platform development

At the core of the solution was a custom-designed gas exchange enclosure that allowed carbon capture testing to occur in a controlled environment. The enclosure integrated with specialized monitoring equipment while maintaining communication with external instrumentation. Pneumatic actuation enabled the enclosure to seal securely over powder-filled testing trays during evaluation cycles.

To automate the oxidation process, a custom misting system was developed that traveled across the powder trays using a pneumatic slide mechanism. This system delivered controlled moisture application while minimizing airflow disturbances that could disrupt the lightweight powder materials.

A Raspberry Pi-based control system was selected to minimize capital costs while providing automation functionality, internet connectivity, VPN access, and onboard I/O capabilities. Although this approach introduced reliability challenges associated with non-industrial hardware, it enabled rapid deployment and process development during the early stages of technology maturation.

Custom Matlab scripts and Excel-based analytical tools were developed to process large datasets generated during testing, allowing researchers to quickly identify trends, compare results, and evaluate process performance across multiple test configurations.

Results

The project successfully transformed a highly manual laboratory process into an automated testing platform capable of supporting significantly higher testing frequency and process development velocity.

The automated system enabled multiple process parameters to be evaluated simultaneously, with complete testing, data collection, and analysis cycles occurring approximately every two days. Individual test campaigns were able to evaluate eight separate test configurations concurrently, dramatically increasing the amount of actionable process data available to the development team.

Key outcomes included:

  • Increased carbon dioxide absorption performance
  • Higher testing throughput and experimental frequency
  • Improved process repeatability and consistency
  • Accelerated process development cycles
  • Simultaneous evaluation of multiple process variables
  • Automated data collection and analysis
  • Improved understanding of powder performance characteristics
  • Identification of improved material formulations

Testing efforts ultimately identified alternative powder materials that delivered improved carbon capture performance while also simplifying post-test handling, disposal, cleaning, and sample preparation activities.

The platform provided Heirloom with a critical bridge between laboratory-scale research and future commercial-scale deployment, allowing the team to rapidly iterate, validate concepts, and identify technologies necessary for larger-scale carbon capture systems.

System Overview

The carbon capture testing platform includes:

  • Custom gas exchange testing enclosure
  • Automated misting and wetting systems
  • Pneumatic actuation systems
  • CO₂ and environmental monitoring instrumentation
  • Humidity and moisture sensing systems
  • Experimental automation controls
  • Remote monitoring capabilities
  • Data acquisition architecture
  • Matlab-based data processing tools
  • Scalable process development infrastructure

Benefits & Impact

  • Accelerated carbon capture process development
  • Increased experimental throughput and testing frequency
  • Improved testing consistency and repeatability
  • Reduced manual labor and operator intervention
  • Enhanced process data collection and analysis
  • Rapid evaluation of multiple process variables
  • Identification of improved material formulations
  • Lower-cost development platform for emerging technology validation
  • Scalable foundation for future production systems
  • Support for commercialization of direct air carbon capture technology

Ready to Partner?

Let’s talk about your unique challenges and how Re:Build DAPR can help you.